Reduced oxygen nanocrystalline materials show improved performance

phys.org | 7/17/2017 | Staff
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Researchers at the University of Connecticut have found that reducing oxygen in some nanocrystalline materials may improve their strength and durability at elevated temperatures, a promising enhancement that could lead to better biosensors, faster jet engines, and greater capacity semiconductors.

"Stabilizing nanocrystals at elevated temperatures is a common challenge," says Peiman Shahbeigi-Roodposhti, a postdoctoral research scholar with UConn's Institute of Materials Science and the study's lead author. "In certain alloys, we found that high levels of oxygen can lead to a significant reduction in their efficiency."

Milling - Process - Glove - Box - Argon

Using a special milling process in an enclosed glove box filled with argon gas, UConn scientists, working in collaboration with researchers from North Carolina State University, were able to synthesize nano-sized crystals of Iron-Chromium and Iron-Chromium-Hafnium with oxygen levels as low as 0.01 percent. These nearly oxygen-free alloy powders appeared to be much more stable than their commercial counterparts with higher oxygen content at elevated temperatures and under high levels of stress.

"In this study, for the first time, optimum oxygen-free nanomaterials were developed," says Sina Shahbazmohamadi, an assistant professor of biomedical engineering at UConn and a co-author on the paper. "Various characterization techniques, including advanced aberration corrected transmission electron microscopy, revealed a significant improvement in grain size stability at elevated temperatures."

Grain - Size - Stability - Scientists - Generation

Grain size stability is important for scientists seeking to develop the next generation of advanced materials. Like fine links in an intricately woven mesh, grains are the small solids from which metals are made. Studies have shown that smaller grains are better when it comes to making stronger and tougher metals...
(Excerpt) Read more at: phys.org
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